- product description
GC-9560-HGHigh purity gas analysis systemSuitable for the detection of trace impurities in high-purity gases such as hydrogen, oxygen, argon, nitrogen, helium, neon, krypton, xenon, carbon dioxide, etc. The instrument is equipped with a highly sensitive helium ionization (PDIHID) detector, using center cutting and blowback technology, and equipped with an injection switching valve and an imported helium purifier with a blowback protection gas path. Through non dead volume sampling or online injection methods, H in the above high-purity gases can be completed in one go2、 O2(Ar)、N2、 CH4、 CO、CO2Common impurities or C1-C4The detection limit for hydrocarbons reaches ppb level, with a repeatability RSD of ≤ 1%.
The national standard GB/T 28726-2012 "Gas Analysis - Helium Ionization Gas Chromatography Method", which was mainly drafted by Hua Ai Chromatography, has been officially announced and implemented since February 1, 2013.
1、 Applicable standards:
GB/T3634.2-2011 "Pure Hydrogen, High Purity Hydrogen, and Ultra Pure Hydrogen" GB/T 14599-2008 "Pure Oxygen, High Purity Oxygen, and Ultra Pure Oxygen"
GB/T 8979-2008 "Pure Nitrogen, High Purity Nitrogen, and Ultra Pure Nitrogen" GB/T 4842-2006 "Argon"
GB/T 4844-2011 "Pure Helium, High Purity Helium, and Ultra Pure Helium" GB/T 17873-1999 "Pure Neon"
GB/T 5829-2006 "Krypton" GB/T 5828-2006 "Xenon"
HG/T 3633-1999 "Pure Methane" GB 10621-2006 "Food Additives - Liquid Carbon Dioxide"
GB/T 23938-2009 "High Purity Carbon Dioxide" GB/T 28125.1-2011 "Determination of Hazardous Substances in Air Separation Processes"
2、 Technical parameters:
1. Detection limit (ppb):
General impurities | ||||||
Types of groceries | H2 | O2(Ar) | N2 | CH4 | CO | CO2 |
inspectmeasurelimit | 5 | 10 | 10 | 5 | 25 | 5 |
hydrocarbon | |||||||
Types of impurities | C2H4 | C2H6 | C3H6 | C3H8 | C4H8 | C4H10 | iC4H10 |
inspectmeasurelimit | 20 | 20 | 20 | 20 | 20 | 20 | 20 |
2. Temperature control indicators:
- Column box: 8 ℃ -400 ℃ at room temperature with an accuracy of ± 0.1 ℃
- Sample injector: Accuracy ± 0.1 ℃ at room temperature between 8 ℃ and 400 ℃
- Detector: Accuracy ± 0.1 ℃ at room temperature between 8 ℃ and 400 ℃
- Temperature control quantity: eight channels
- Program heating: 8th order
- Heating rate: 1 ℃~40 ℃
- Cooling rate: within 7 minutes (350 ℃ to 50 ℃)
3. Helium ionization detector (PDD):
- Discharge mode: Pulse discharge
- Baseline noise: ≤ 0.1mv
- Baseline drift: ≤ 0.5mv/30min
- Detection limit: ≤ 1.0 × 10-10g/ml
4. Carrier gas purifier:
- Purified gases: He, Ar, Ne, Kr, Xe, Rn
- Maximum operating pressure: 1000Psi
- Gas removal: H2、 O2, N2, CO, CO2, CH4, H2O, NO, NH3, CF4, etc
- Residual concentration: ≤ 10pppb
5. Workstation performance:
- Communication interface: RS232/USB interface
- High precision: 24 bit high-precision A/D
- Resolution: ± 1UV
- Input voltage range: -5mv to+1v
- Sampling frequency: maximum 20 times/second
- Dynamic range: 106
- Integral sensitivity: 1 μ v • sec
- Linearity:<± 0.1%.
- Reproducibility: 0.06%.
6. Other parameters: size, weight, power supply:
- Dimensions: Width 655mm x Height 500mm x Depth 480mm
- Weight:~48kg
- Power supply: 220V ± 22V, 50Hz, power ≥ 2kW
3、 System configuration:
(1) GC-9560-HG High Purity Gas Analysis System (2) Helium Ionization Detector (PDHID)
(3) Central cutting system (4) multi column box system
(5) Helium Purifier (6) Standard Gas
(7) Chromatography Column (9) Oxygen Adsorption and Reduction System
(10) Special pressure reducing valve for carrier gas (11), no dead volume dedicated sampling valve
(12) GC-9560V4.0 Reverse Chromatography Workstation